移动加热源法制备单层硒化镓晶体

为了解决硒化镓(GaSe)晶体制备困难、化学性能差的问题,对GaSe晶体传统的化学汽相沉积制备方法进行了改进,采用移动加热源法制备GaSe晶体。搭建了GaSe晶体的制备装置,通过单片机精确调控制备晶体的高温炉的加热温度、移动位置等参数,并采用光学显微镜和原子力显微镜对所制备的GaSe晶体进行辅助表征。研究表明,利用移动加热源法可以制备出表面光滑且尺寸较大的单层二维GaSe晶体。由于对机电设备实现了自动精密移动,可对单层二维GaSe晶体实现高质量大批量的制备,有利于GaSe晶体在光电子学和纳电子学中的广泛应用。     

淮河入江水道行洪能力分析

入江水道是淮河下游最大的泄洪河道,承担着淮河上中游70%以上的洪水泄入长江。根据1961—2018年大洪水期间的实测资料,利用水位流量法计算分析入江水道的泄洪能力和防洪能力。结果表明:因历史客观条件限制以及4个梯级控制河段整治的难度与复杂性,在不同时期各控制河段的行洪能力呈现各自不同的特点;经过多年持续有效治理,河道行洪能力整体得到提高;由近年来实测资料推算,各控制河段的行洪能力基本达到设计要求。对入江水道行洪能力的分析为淮河下游区的防汛抗洪和降低特大洪水威胁提供借鉴和参考,对区域经济社会又好又快发展具有现实意义。     

环氧丙烷产业现状及发展趋势

简述了全球及我国环氧丙烷产业的生产及供需现状;对环氧丙烷在聚醚多元醇、丙二醇/碳酸二甲酯、丙二醇醚及其酯类等领域的应用进行了分析;并对环氧丙烷生产技术进行了比较,提出了发展建议。     

Gold Drugs with {Au(PPh3)}+ Moiety: Advantages and Medicinal Applications

Following the success of Auranofin as an anti-arthritic drug, search for novel gold drugs has afforded a large number of [L−Au(PPh₃)] complexes that exhibit notable salutary effects. Unlike Au(III)-containing species, these gold complexes with {Au(PPh₃)}⁺ moiety are stable in biological media and readily exchange L with S- and Se-containing enzymes or proteins. Such exchange leads to rapid reduction of microbial loads or induction of apoptotic cell death at malignant sites. In many cases the lipophilic {Au(PPh₃)}⁺ moiety delivers a desirable toxic L to the specific cellular target in addition to exhibiting its own beneficial activity. Further research and utilization of this synthon in drug design could lead to novel chemotherapeutics for treatment of drug-resistant pathogens and cancers.     

Identification of factors that accelerate hydrogen production by Clostridium butyricum RAK25832 using casamino acids as a nitrogen source

The ability of Clostridium butyricum RAK25832 to use casamino acids as a nitrogen source was investigated. Strain RAK25832 showed the capacity to utilize different types of carbon sources. With glucose as a carbon source (10 g/L), the preferred final concentration of casamino acids was 26.67 g/L, with a cumulative hydrogen production, production rate, and yield of 2505 mL H₂/L, 160 mL/h, and 1.81 mol H₂/mol glucose, respectively. Eighteen metal elements were screened to identify the most important metals for biohydrogen production, and four elements were optimized. The optimal medium composition was MgCl₂·6H₂O (0.1 g/L), K₂HPO₄·3H₂O (6.67 g/L), NaHCO₃ (2.6 g/L), and FeCl₂·4H₂O (0.002 g/L). Vitamin supplementation of the medium showed no significant effect on hydrogen production. Under the optimized conditions, cumulative hydrogen production reached 3074 mL H₂/L. This is the first study to demonstrate the use of casamino acids as a nitrogen source by C. butyricum.     

苏里格南区气井井筒堵塞原因分析与防治对策

针对苏里格南区气井井筒特别是油管内形成大量堵塞物现状,通过现场调研和室内研究,明确气井井筒堵塞原因,并提出相应的防治对策。     

特厚煤层综放工作面瓦斯抽采技术研究

为解决蒋家河煤矿采空区瓦斯涌出量大、上隅角瓦斯超限和回风平巷风排瓦斯量大等问题,提出了本煤层预抽、专用瓦斯抽放巷抽采和上隅角埋管抽采瓦斯相结合的方法对该矿ZF202综放工作面进行瓦斯治理,进行了现场实测和瓦斯抽采效果分析。结果表明,本煤层预抽后,瓦斯含量由7.92 m^3/t下降为4.21 m^3/t,瓦斯压力由0.72 MPa下降为0.38 MPa;上隅角瓦斯浓度由0.78%下降至0.4%左右。通过对比,专用瓦斯抽放巷的抽采纯量是高位钻孔的2.5倍,抽采效果好于高位钻孔,使工作面和上隅角瓦斯浓度保持较低水平,有效地解决了特厚煤层综放工作面瓦斯超限问题,为安全生产提供了重要保障。     

全面采矿法在小矿体开采中的应用

介绍了黄背场铅锌矿采用全面采矿法在小矿体开采和探矿中的应用实践,该工艺具有投入少、生产成本低,简单易行等特点,有很强的适应性和实用性。     

美国大数据战略及对我国启示

美国当前在大数据方面全球领先。2010年奥巴马将发展大数据上升为国家战略,建立了一系列负责大数据的专门机构,发布大量相关战略性文件和法令。大数据在美国各个领域得到广泛应用,并基本成体系。当前我国大数据发展取得进步但仍存在问题,借鉴美国大数据战略的具体做法可为完善我国大数据战略提供较好的参考价值。     

自动电位滴定仪示值误差测量不确定度评定

按照JJG 814-2015规定,自动电位滴定仪需进行电计示值误差和仪器示值误差检定,本文例举对这两项检定结果进行不确定度评定,供相关人员参考。